Back to Search Start Over

Effect of Calcination on Characteristics of Nickel Ferrite Nanoparticles Synthesized by Sol-Gel Method

Effect of Calcination on Characteristics of Nickel Ferrite Nanoparticles Synthesized by Sol-Gel Method

Authors :
Pérez, E.
Márquez, Gerson
Sagredo, Vicente
Publication Year :
2019
Publisher :
Zenodo, 2019.

Abstract

Nanosized nickel ferrite compound was synthesized by using sol-gel method. Significant differences in the particle size were obtained after two different calcination cycles at 873 and 1073 K. The average particle size of sample calcinated at 873K was found to be 25 nm which increases up to 120 nm on calcination at 1073 K. Low-field magnetization data show at room temperature an strong irreversibility between zero field cooled(ZFC) and field cooled(FC) cycles without a clear blocking temperature. The FC data shows a behavior typical for strongly coupled system because of the interaction particle-particle favored by the agglomeration of particles observed by the SEM micrographs. The effective magnetic moment per molecule evaluated from hysteresis loops at magnetic field of 5.5 Tesla is slightly smaller than 2 μB.<br />{"references":["J. Wang et al., \"Synthesis and magnetic properties of Zn1-xMnxFe2O4 nanoparticles\", Physica B: Cond. Matt., 349(1-4) (2004) 124- 128.","J.G. Duque et al., \"Magnetic properties of NiFe2O4, nanoparticles produced by a new chemical method\", Physica B: Cond. Matt., 398(1-2) (2007) 287-290.","D.S. Mathew and R.-S. Juang, \"An overview of the structure and magnetism of spinel ferrite nanoparticles and their synthesis in microemulsions\", Chem. Eng. J., 129(1-3) (2007) 51-65.","J.L. Gunjakar, A.M. More, K.V. Gurav and C.D. Lokhande, \"Chemical synthesis of spinel nickel ferrite (NiFe2O4) nano-sheets\", Appl. Surf. Sci., 254(18) (2008) 5844-5848.","A. Baykal, N. Kasapoglu, Y. Koseoglu, M. Toprak and H. Bayrakdar, \"CTAB-assisted hydrothermal synthesis of NiFe2O4 and its magnetic characterization\", J. Alloys Compd., 464(1-2) (2008) 514-518.","F.S. Tehrani, V. Daadmehr, A.T. Rezakhani, R.H. Akbarnejad and S. Gholipour, \"Structural, magnetic, and optical properties of zinc- and copper- substituted nickel ferrite nanocrystals\", J. Supercond. Nov. Mag., 25(7) (2012) 2443- 2455.","G. Dixit, J.P. Singh, R.C. Srivastava, H.M. Agrawal and R.J. Chaudhary, \"Structural, magnetic and optical studies of nickel ferrite thin films\", Adv. Mat. Lett., 3(1) (2012) 21-28.","A. Alarifi, N.M. Deraz and S. Shaban, \"Structural, morphological and magnetic properties of NiFe2O4 nano-particles\", J. Alloys Compd., 486(1-2) (2009) 501-506.","S. Prasad and N.S. Gajbhiye, \"Magnetic studies of nanosized nickel ferrite particles synthesized by the citrate precursor technique\", J. Alloys Compd., 265(1-2) (1998) 87-92.","H. R. Dehghanpour, \"Physical and Chemical Properties of NiFe2O4 Nanoparticles Prepared by Combustion and Ultrasonic Bath Methods\", Russian J. Appl. Chem., 89(1) (2016) 80-83.","I.A. Abdel-Latif, \"Fabrication of Nano-Size Nickel Ferrites for Gas Sensors Applications\", J. Phys., 1(2) (2012) 50-53.","Y. Shi, J. Ding, X. Liu and J. Wang, \"NiFe2O4 ultrafine particles prepared by coprecipitation/mechanical alloying\", J. Magn. Magn. Mater., 205(2-3) (1999) 249-254.","X. Tan, G. Li, Y. Zhao and C. Hu, \"Effect of Cu content on the structure of Ni1-xCuxFe2O4 spinels\", Mater. Res. Bull., 44 (2009) 2160- 2168.","K. Nejati and R. Zabihi, \"Preparation and magnetic properties of nano size nickel ferrite particles using hydrothermal method\", Chem. Centr. J., 6 (2012) 23-28.","M. Salavati-Niasari, F. Davar and T. Mahmoudi, \"A simple route to synthesize nanocrystalline nickel ferrite (NiFe2O4) in the presence of octanoic acid as a surfactant\", Polyhedron, 28(8) (2009) 1455-1458.","K. Maaz, S. Karim, A. Mumtaz, S.K. Hasanain, J. Liu and J.L. Duan, \"Synthesis and magnetic characterization of nickel ferrite nanoparticles prepared by coprecipitation route\", J. Magn. Magn. Mater., 321(12) (2009) 1838-1842.","H. Kavas, N. Kasapoglu, A. Baykal and Y. Kaseoglu, \"Characterization of NiFe2O4 nanoparticles synthesized by various methods\", Chem. Papers., 63(4) (2009) 450-455.","H. Nathani, S. Gubbala and R.D.K. Misra, \"Magnetic behavior of nanocrystalline nickel ferrite: Part I. The effect of surface roughness\", Mater. Sci. Eng. B, 121(1-2) (2005) 126-136.","P. Sivakumar, R. Ramesh, A. Ramanand, S. Ponnusamy and C. Muthamizhchelvan, \"Synthesis and characterization of NiFe2O4 nanoparticles and nanorods\", J. Alloys Comp., 563 (2013) 6-11.","R.H. Kodama, A.E. Berkowitz, J.E.J. McNiff and S. Foner, \"Surface Spin Disorder in NiFe2O4 Nanoparticles\", Phys. Rev. Lett., 77(2) (1996) 394-397.","H. Nathani and R.D.K. Misra, \"Surface effects on the magnetic behavior of nanocrystalline nickel ferrites and nickel ferrite-polymer nanocomposites\", Mater. Sci. Eng. B, 113(3) (2004) 228-235.","A.B. Nawale, N.S. Kanhe, K.R. Patil, S.V. Bhoraskar, V.L. Mathe and A.K. Das, \"Magnetic properties of thermal plasma synthesized nanocrystalline nickel ferrite (NiFe2O4)\", J. Alloys Compd., 509(12) (2011) 4404-4413.","A. Pradeep, P. Priyadharsini and G. Chandrasekaran, \"Production of single phase nano size NiFe2O4 particles using sol-gel auto combustion route by optimizing the preparation conditions\", Mater. Chem. Phys., 112(2) (2008) 572-576.","Yu.A. Mirgorod, N.A. Borshch, V.M. Fedosyuk and G.Yu. Yurkov, \"Magnetic Properties of Nickel Ferrite Nanoparticles Prepared Using Flotation Extraction\", Inorg. Mater., 49(1) (2013) 109-113.","Z. Shi, J. Zhang, D. Gao, Z. Zhu, Z. Yang, Z. Zhang and D. Xue, \"Magnetic resonance of the NiFe2O4 nanoparticles in the gigahertz range\", Nanoscale Res. Lett., 8 (2013) 404-408.","S. Mitra, K. Mandal and P. Anil Kumar, \"Temperature dependence of magnetic properties of NiFe2O4 nanoparticles embeded in SiO2 matrix\", J. Magnet. Mag. Mater., 306(2) (2006) 254-259.","Y. Cheng et al., \"Synthesis and magnetic properties of nickel ferrite nano-octahedra\", J. Solid State Chem., 178(7) (2005) 2394-2397.","L.A. Garcia-Cerda and S.M. Montemayor, \"Synthesis of CoFe2O4 nanoparticles embedded in a silica matrix by the citrate precursor technique\", J. Magnet. Mag. Mater., 294(2) (2005) e43-e46.","S. Maensiri et al., \"A simple route to synthesize nickel ferrite NiFe2O4 nanoparticles using egg white\", Scripta Materialia, 56(9) (2007) 797-800."]}

Details

Language :
English
Database :
OpenAIRE
Accession number :
edsair.doi.dedup.....858884900d9f90aaa3ec28b214fe8d6b
Full Text :
https://doi.org/10.5281/zenodo.7979409