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Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy
- Source :
- Spectrochimica acta. Part B, Atomic spectroscopy 194 (2022): 106482-1–106482-10. doi:10.1016/j.sab.2022.106482, info:cnr-pdr/source/autori:Simona Raneri, Asia Botto, Beatrice Campanella, Milos Momcilovic, Vincenzo Palleschi, Francesco Poggialini, Claudia Sciuto, Gabriele Gattiglia, Francesco Volpintesta, Thirumalini Selvaraj Sanja Zivkovic, Giulia Lorenzetti, Stefano Legnaioli/titolo:Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy/doi:10.1016%2Fj.sab.2022.106482/rivista:Spectrochimica acta. Part B, Atomic spectroscopy/anno:2022/pagina_da:106482-1/pagina_a:106482-10/intervallo_pagine:106482-1–106482-10/volume:194, Spectrochimica Acta. Part B: Atomic Spectroscopy
- Publication Year :
- 2022
- Publisher :
- Elsevier BV, 2022.
-
Abstract
- Laser-Induced Breakdown Spectroscopy (LIBS) micro-mapping is an important analytical tool for the study of geomaterials. In this work, this technique was applied, for the first time, to the analysis of alkali-activated materials and geopolymers, as well as rocks, mortars and bricks. The results obtained were compared with the ones obtained using Energy-Dispersive X-Ray Fluorescence (ED-XRF) macro-mapping and the advantages of the LIBS approach (speed, lateral and in-depth resolution, capability of light elements analysis) were highlighted. The issues associated with the quantitative determination of the samples' composition from the analysis of the LIBS spectra were also briefly discussed.
- Subjects :
- XRF macro-mapping
Geopolymers
Geomaterials
CF-LIBS
LIBS micro-mapping XRF macro-mapping Geomaterials Alkali-activated materials Geopolymers CF-LIBS K-means
Atomic and Molecular Physics, and Optics
Analytical Chemistry
LIBS micro-mapping, XRF macro-mapping, geomaterials, alkali-activated materials, geopolymers, CF-LIBS, K-means
geomaterials
geopolymers
Alkali-activated materials
LIBS micro-mapping
alkali-activated materials
K-means
Instrumentation
Spectroscopy
Subjects
Details
- ISSN :
- 05848547
- Volume :
- 194
- Database :
- OpenAIRE
- Journal :
- Spectrochimica Acta Part B: Atomic Spectroscopy
- Accession number :
- edsair.doi.dedup.....844ae0f0ebdfa3205cbb63994ef56b8c