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Low-budget 3D-printed equipment for continuous flow reactions

Authors :
Thomas Klein
Jochen M. Neumaier
Amiera Madani
Thomas Ziegler
Source :
Beilstein Journal of Organic Chemistry, Beilstein Journal of Organic Chemistry, Vol 15, Iss 1, Pp 558-566 (2019)
Publication Year :
2019
Publisher :
Beilstein Institut, 2019.

Abstract

This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series.

Details

ISSN :
18605397
Volume :
15
Database :
OpenAIRE
Journal :
Beilstein Journal of Organic Chemistry
Accession number :
edsair.doi.dedup.....753d31f6018db50ec41029648d701e7c