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Preliminary results of CoQtz-N: A quartz reference material for terrestrial in-situ cosmogenic 10Be and 26Al measurements

Authors :
L. Leanni
F. von Blanckenburg
Stewart P.H.T. Freeman
A. Dewald
David Fink
Steven A. Binnie
Tibor Dunai
Aster Team
Kristina Hippe
Sheng Xu
Derek Fabel
Reka H Fulop
L.K. Fifield
Ralf Hetzel
Susan Ivy-Ochs
Elena Voronina
Stefan Heinze
Andrew S. Hein
Hella Wittmann
Naki Akçar
Colin Maden
Toshiyuki Fujioka
Mirjam Schaller
Christoph Vockenhuber
Klaus M. Wilcken
M. Christl
Cornelia Spiegel
Source :
Nuclear Instruments and Methods in Physics Research / B, Binnie, S A, Dewald, A, Heinze, S, Voronina, E, Hein, A, Wittmann, H, Von Blanckenburg, F, Hetzel, R, Christl, M, Schaller, M, Léanni, L, Aster Team, Hippe, K, Vockenhuber, C, Ivy-ochs, S, Maden, C, Fülöp, R, Fink, D, Wilcken, K M, Fujioka, T, Fabel, D, Freeman, S P H T, Xu, S, Fifield, L K, Akçar, N, Spiegel, C & Dunai, T J 2019, ' Preliminary results of CoQtz-N: A quartz reference material for terrestrial in-situ cosmogenic 10Be and 26Al measurements ', Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms . https://doi.org/10.1016/j.nimb.2019.04.073
Publication Year :
2019

Abstract

There is growing interest in geochronological applications of terrestrial in situ-produced cosmogenic nuclides, with the most commonly measured being 10Be and 26Al in quartz. To extract and then separate these radionuclides from quartz and prepare them in the oxide form suitable for accelerator mass spectrometry (AMS) requires extensive and careful laboratory processing. Here we discuss the suitability of a crushed, sieved and etched, sub-aerially exposed vein quartz specimen (CoQtz-N) to act as a reference material for chemical laboratory preparation and AMS measurements. Splits of CoQtz-N were distributed to eleven target preparation laboratories. The CoQtz-N 10Be targets were then measured at seven different AMS facilities and five of the preparation laboratories had their 26Al targets measured at four different AMS facilities. We show that CoQtz-N splits are sufficiently homogeneous with regard to nuclide concentrations, that it has been cleaned of any atmospheric derived (i.e. meteoric) 10Be and that it has low concentrations of the major elements that can interfere with Be and Al extraction chemistry and AMS measurements. We derive preliminary concentrations for 10Be and 26Al in CoQtz-N as 2.53 ± 0.09 × 106 at/g and 15.6 ± 1.6 × 106 at/g, respectively, at the 95% confidence limit.

Details

Database :
OpenAIRE
Journal :
Nuclear Instruments and Methods in Physics Research / B, Binnie, S A, Dewald, A, Heinze, S, Voronina, E, Hein, A, Wittmann, H, Von Blanckenburg, F, Hetzel, R, Christl, M, Schaller, M, Léanni, L, Aster Team, Hippe, K, Vockenhuber, C, Ivy-ochs, S, Maden, C, Fülöp, R, Fink, D, Wilcken, K M, Fujioka, T, Fabel, D, Freeman, S P H T, Xu, S, Fifield, L K, Akçar, N, Spiegel, C & Dunai, T J 2019, ' Preliminary results of CoQtz-N: A quartz reference material for terrestrial in-situ cosmogenic 10Be and 26Al measurements ', Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms . https://doi.org/10.1016/j.nimb.2019.04.073
Accession number :
edsair.doi.dedup.....7422e7bc7e559a9ac67c98c960818752
Full Text :
https://doi.org/10.1016/j.nimb.2019.04.073