Back to Search
Start Over
Levitation apparatus for neutron diffraction investigations on high temperature liquids
- Source :
- Review of Scientific Instruments, Review of Scientific Instruments, American Institute of Physics, 2006, 77 (5), pp.053903. ⟨10.1063/1.2200756⟩
- Publication Year :
- 2006
- Publisher :
- AIP Publishing, 2006.
-
Abstract
- We describe a new high temperature environment based on aerodynamic levitation and laser heating designed for neutron scattering experiments up to 3000°C. The sample is heated to the desired temperature with three CO2 lasers from different directions in order to obtain a homogeneous temperature distribution. The apparent temperature of the sample is measured with an optical pyrometer, and two video cameras are employed to monitor the sample behavior during heating. The levitation setup is enclosed in a vacuum-tight chamber, enabling a high degree of gas purity and a reproducible sample environment for structural investigations on both oxide and metallic melts. High-quality neutron diffraction data have been obtained on liquid Y3Al5O12 and ZrNi alloy for relatively short counting times (1.5h).
- Subjects :
- Materials science
Neutron diffraction
Alloy
Oxide
02 engineering and technology
Neutron scattering
engineering.material
7. Clean energy
01 natural sciences
Aerodynamic levitation
law.invention
chemistry.chemical_compound
Optics
law
0103 physical sciences
010306 general physics
Instrumentation
ComputingMilieux_MISCELLANEOUS
Pyrometer
business.industry
Zirconium alloy
021001 nanoscience & nanotechnology
chemistry
[PHYS.COND.CM-MS]Physics [physics]/Condensed Matter [cond-mat]/Materials Science [cond-mat.mtrl-sci]
Levitation
engineering
0210 nano-technology
business
Subjects
Details
- ISSN :
- 10897623 and 00346748
- Volume :
- 77
- Database :
- OpenAIRE
- Journal :
- Review of Scientific Instruments
- Accession number :
- edsair.doi.dedup.....66aabf5925bf1de843c85efe89c2d172