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Light-irradiation at 700 MPa down to 1.5 K for neutron diffraction

Authors :
Philippe Guionneau
Claude Payre
Jean Luc Laborier
Paraskevas Parisiades
Marie-Hélène Lemée-Cailleau
Jean Paul Gonzales
Eddy Lelièvre-Berna
J. P. Bidet
Patrick Rosa
European Synchrotron Radiation Facility (ESRF)
Institut Laue-Langevin (ILL)
ILL
Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB)
Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS)-Institut Polytechnique de Bordeaux-Université de Bordeaux (UB)
ANR-09-BLAN-0175-04
Source :
Measurement Science and Technology, Measurement Science and Technology, IOP Publishing, 2016, 27 (4), pp.047001. ⟨10.1088/0957-0233/27/4/047001⟩
Publication Year :
2016
Publisher :
IOP Publishing, 2016.

Abstract

International audience; We present a new continuously-loaded high-pressure cell for neutron diffraction made from TiZr 'null-matrix' alloy that combines high mechanical resistance below 100 °C and negligible coherent neutron scattering. This cell operates at a maximum pressure of 700 MPa down to a temperature of 1.5 K. A sapphire optical window allows simultaneous illumination of the sample over the broad wavelength range ~0.4 to almost 5 μm. The pressure is applied with Fluorinert or helium gas to ensure the best possible hydrostatic conditions at cryogenic temperatures.

Details

Language :
English
ISSN :
09570233 and 13616501
Database :
OpenAIRE
Journal :
Measurement Science and Technology, Measurement Science and Technology, IOP Publishing, 2016, 27 (4), pp.047001. ⟨10.1088/0957-0233/27/4/047001⟩
Accession number :
edsair.doi.dedup.....666926362dd6f519af383259737b227c
Full Text :
https://doi.org/10.1088/0957-0233/27/4/047001⟩