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Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS
- Source :
- Chemical Communications, Chemical communications (Cambridge, England), Chemical Communications, Royal Society of Chemistry, 2018, 54 (65), pp.8972-8975. ⟨10.1039/c8cc04437f⟩, Chemical Communications 54 (2018), Nr. 65
- Publication Year :
- 2018
-
Abstract
- Fast (>100 kHz) magic angle spinning solid-state NMR allows combining high-sensitive proton detection with the absence of an intrinsic molecular weight limit. Using this technique we observe for the first time narrow 1H RNA resonances and assign nucleotide spin systems with only 200 μg of uniformly 13C,15N-labelled RNA.
- Subjects :
- RNA Resonance
Dewey Decimal Classification::500 | Naturwissenschaften::540 | Chemie
Materials science
Proton
Nuclear Magnetic Resonance
010402 general chemistry
01 natural sciences
Catalysis
Nuclear magnetic resonance
[CHIM.ANAL]Chemical Sciences/Analytical chemistry
Materials Chemistry
Magic angle spinning
Rapid access
Spectroscopy
ComputingMilieux_MISCELLANEOUS
Spin-½
010405 organic chemistry
Metals and Alloys
RNA
General Chemistry
0104 chemical sciences
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Solid-state nuclear magnetic resonance
ddc:540
Ceramics and Composites
Subjects
Details
- ISSN :
- 13597345 and 1364548X
- Database :
- OpenAIRE
- Journal :
- Chemical Communications
- Accession number :
- edsair.doi.dedup.....5c34e72fadb5c9ea8a043c6a106eada2
- Full Text :
- https://doi.org/10.1039/c8cc04437f