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A preferred orientation correction to describe a fiber texture under glancing incidence

Authors :
Dominique Gosset
David Simeone
Gianguido Baldinozzi
Laboratoire Structures, Propriétés et Modélisation des solides (SPMS)
Institut de Chimie du CNRS (INC)-CentraleSupélec-Centre National de la Recherche Scientifique (CNRS)
Laboratoire d'Analyse Microstructurale des Matériaux (LA2M)
Service des Recherches Métallurgiques Appliquées (SRMA)
Département des Matériaux pour le Nucléaire (DMN)
CEA-Direction des Energies (ex-Direction de l'Energie Nucléaire) (CEA-DES (ex-DEN))
Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay-CEA-Direction des Energies (ex-Direction de l'Energie Nucléaire) (CEA-DES (ex-DEN))
Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay-Département des Matériaux pour le Nucléaire (DMN)
Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay
RTRA Triangle de la physique, projet 2011-074T, INSTRUMAT. C'nano Ile-de-France, projet SolNac (2009)
Source :
Journal of Applied Crystallography, Journal of Applied Crystallography, International Union of Crystallography, 2013, 46 (1), pp.93-98. ⟨10.1107/S0021889812045736⟩, Journal of Applied Crystallography, 2013, 46 (1), pp.93-98. ⟨10.1107/S0021889812045736⟩
Publication Year :
2013
Publisher :
HAL CCSD, 2013.

Abstract

International audience; Much work is nowadays being devoted to the characterization of the structure and the microstructure of thin films and mesoporous materials. Different physical and chemical processes used to elaborate these thin films often induce a fiber texture in these materials. The X-ray glancing-incidence technique appears to be a useful tool for collecting diffraction patterns of thin films while avoiding the peaks of the substrate. However, the scattering vector in this asymmetric scattering geometry is not perpendicular to the surface of the sample. This point implies that the correction developed to model the effects of a fiber texture in Bragg-Brentano geometry, where the scattering vector is always normal to the surface of the sample, cannot be applied in glancing incidence. This work presents a procedure to correct the preferred orientation due to this fiber texture in asymmetric scattering geometry and then in glancing incidence. By an example, it is proved that this correction of the fiber texture is efficient. The main point of interest regarding this correction is that only a few parameters are needed to handle the effect of the fiber texture on the diffraction patterns collected in asymmetric scattering geometry and then under glancing incidence.

Details

Language :
English
ISSN :
00218898 and 16005767
Database :
OpenAIRE
Journal :
Journal of Applied Crystallography, Journal of Applied Crystallography, International Union of Crystallography, 2013, 46 (1), pp.93-98. ⟨10.1107/S0021889812045736⟩, Journal of Applied Crystallography, 2013, 46 (1), pp.93-98. ⟨10.1107/S0021889812045736⟩
Accession number :
edsair.doi.dedup.....56536c4e6ea3ffc0d6ba5cfcaa855427
Full Text :
https://doi.org/10.1107/S0021889812045736⟩