Influence of temperature change on microstructure evolution in Ni alloys irradiated with neutrons

To investigate the microstructure evolution during temperature change irradiation, Ni and its binary alloys were irradiated in the Japan Materials Testing Reactor to doses up to 0.46 dpa under two cycles of temperature change of 533/693 K, i.e., 533 K, then 693 K, then 533 K, then 693 K. The irradiation dose at each temperature stage was about the same. The specimen sets were pulled out five times during irradiation. In the beginning of the first irradiation at the high temperature of 693 K after irradiation at 533 K, the densities of interstitial type dislocation loops and voids decreased in pure Ni, Ni–2at.%Cu and Ni–2at.%Ge alloys. In the second irradiation at 533 K, however, the formation of dislocation loops and voids was promoted. The void density continued to increase even after the second irradiation at 693 K. On the other hand, in Ni–2at.%Si and Ni–2at.%Sn alloys, where the formation of voids was suppressed by addition of the minor elements Si or Sn, the microstructure evolution was almost independent of irradiation temperature.