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Flexible Drift Tube for High Resolution Ion Mobility Spectrometry (Flex-DT-IMS)

Authors :
Iain S. Young
Tirayut Vilaivan
Simon Maher
Cedric Boisdon
Barry L. Smith
Thanit Praneenararat
Source :
Analytical Chemistry
Publication Year :
2020
Publisher :
American Chemical Society (ACS), 2020.

Abstract

This paper describes, in detail, the development of a novel, low-cost, and flexible drift tube (DT) along with an associated ion mobility spectrometer system. The DT is constructed from a flexible printed circuit board (PCB), with a bespoke “dog-leg” track design, that can be rolled up for ease of assembly. This approach incorporates a shielding layer, as part of the flexible PCB design, and represents the minimum dimensional footprint conceivable for a DT. The low thermal mass of the polyimide substrate and overlapping electrodes, as afforded by the dog-leg design, allow for efficient heat management and high field linearity within the tube–achieved from a single PCB. This is further enhanced by a novel double-glazing configuration which provides a simple and effective means for gas management, minimizing thermal variation within the assembly. Herein, we provide a full experimental characterization of the flexible DT ion mobility spectrometer (Flex-DT-IMS) with corresponding electrodynamic (Simion 8.1) and fluid dynamic (SolidWorks) simulations. The Flex-DT-IMS is shown to have a resolution >80 and a detection limit of low nanograms for the analysis of common explosives (RDX, PETN, HMX, and TNT).

Details

ISSN :
15206882 and 00032700
Volume :
92
Database :
OpenAIRE
Journal :
Analytical Chemistry
Accession number :
edsair.doi.dedup.....5366e65512de9084b1a372b4ef2e8d3c
Full Text :
https://doi.org/10.1021/acs.analchem.0c01357