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Koenigs–Knorr reaction of fusel alcohols with methyl (1-bromo-2,3,4-tri-O-acetyl-α-d-glucopyranosid)uronate leading to the protected alkyl glucuronides—crystal structures and high resolution 1H and 13C NMR data

Authors :
Franziska Emmerling
Antje Gebert
Bettina Mönch
Irene Nehls
Roland Becker
Source :
Carbohydrate Research. 352:186-190
Publication Year :
2012
Publisher :
Elsevier BV, 2012.

Abstract

Crystal structures and high resolution 1H and 13C NMR spectral data for methyl (alkyl 2,3,4-tri-O-acetyl-β- d -glucopyranosid)uronates (alkyl = methyl, ethyl, n-propyl, i-propyl, n-butyl, sec-butyl, i-butyl, n-pentyl, 2-methyl-1-butyl and 3-methyl-1-butyl) are presented.

Details

ISSN :
00086215
Volume :
352
Database :
OpenAIRE
Journal :
Carbohydrate Research
Accession number :
edsair.doi.dedup.....4ff410abc1097ee5d2ab9acdd8f4a643
Full Text :
https://doi.org/10.1016/j.carres.2012.01.002