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Design and performance of an automated chemical extraction bench for the preparation of 10Be and 26Al targets to be analyzed by accelerator mass spectrometry
- Source :
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2019, 456, pp.230-235. ⟨10.1016/j.nimb.2019.04.002⟩, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Elsevier, 2019, 456, pp.230-235. ⟨10.1016/j.nimb.2019.04.002⟩, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Elsevier, 2019, ⟨10.1016/j.nimb.2019.04.002⟩
- Publication Year :
- 2019
- Publisher :
- HAL CCSD, 2019.
-
Abstract
- International audience; The growing number of studies based on data provided by the accelerator mass spectrometry (AMS) technique from increasingly diverse matrices implies that developing very effective and reproducible sample processing techniques is crucial to meet the demand generated. After being dissolved, the isolation of the cosmogenic nuclide to be measured and its chemical purification imply complex processes throughout successive stages The presented automatic system was designed to perform the final steps of the Be-10 and Al-26 chemical extraction protocol from natural matrices (sediments, pure mineral phases, ...), previously purified, decontaminated and dissolved in the case of in situ-produced cosmogenic nuclides, or leached or dissolved in the case of meteoric cosmogenic nuclides. Driven by Labview software, the developed automatic system, in addition to freeing the operator from tedious tasks, allows reproducibly processing simultaneously up to eight samples of different volumes in roughly 40 min. This article presents the design of the automated extraction bench and its performance based on the recovery efficiency of the stable element and the reproducibility of the measurements of the cosmogenic nuclide concentrations by AMS.
- Subjects :
- [SDU.STU.TE]Sciences of the Universe [physics]/Earth Sciences/Tectonics
Nuclear and High Energy Physics
010504 meteorology & atmospheric sciences
business.industry
[SDE.MCG]Environmental Sciences/Global Changes
Sample processing
Extraction (chemistry)
Labview software
Stable element
010502 geochemistry & geophysics
01 natural sciences
automated bench
Environmental science
cosmogenic preparation
[SDU.STU.GM]Sciences of the Universe [physics]/Earth Sciences/Geomorphology
Cosmogenic nuclide
Process engineering
business
labview
[SDU.ENVI]Sciences of the Universe [physics]/Continental interfaces, environment
Instrumentation
ComputingMilieux_MISCELLANEOUS
0105 earth and related environmental sciences
Accelerator mass spectrometry
Subjects
Details
- Language :
- English
- ISSN :
- 0168583X
- Database :
- OpenAIRE
- Journal :
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2019, 456, pp.230-235. ⟨10.1016/j.nimb.2019.04.002⟩, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Elsevier, 2019, 456, pp.230-235. ⟨10.1016/j.nimb.2019.04.002⟩, Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Elsevier, 2019, ⟨10.1016/j.nimb.2019.04.002⟩
- Accession number :
- edsair.doi.dedup.....3dbce6af337fa95f13bdda060eba4c8a
- Full Text :
- https://doi.org/10.1016/j.nimb.2019.04.002⟩