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Ultrahigh-resolution NMR spectroscopy

Authors :
Nicola J Meharry
Ralph W. Adams
Damien Jeannerat
Mathias Nilsson
Mohammadali Foroozandeh
Gareth A. Morris
Source :
Angewandte Chemie (International Ed. in English), Angewandte Chemie: International Edition, Vol. 53, No 27 (2014) pp. 6990-6992
Publication Year :
2014

Abstract

All psyched up: A flexible and general pure shift experiment (PSYCHE) has been developed that offers superior sensitivity, spectral purity, and tolerance of strong coupling over existing methods for broadband homonuclear decoupling. The partial spectra of estradiol in [D6]DMSO obtained by normal 1H NMR spectroscopy and PSYCHE are shown for comparison.

Details

ISSN :
15213773 and 14337851
Volume :
53
Issue :
27
Database :
OpenAIRE
Journal :
Angewandte Chemie (International ed. in English)
Accession number :
edsair.doi.dedup.....2067c69d8ffad8733e563bbb6fa41a4f