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Morphology-Controlled Synthesis Of SrTiO3 Nanocube By Capping Agent-Assisted Solvothermal Method
- Source :
- Molekul, Vol 11, Iss 1, Pp 25-32 (2016)
- Publication Year :
- 2016
- Publisher :
- Jenderal Soedirman University, 2016.
-
Abstract
- The synthesis of SrTiO3 nanocubes have been carried out by solvothermal process using cetyl trimethyl ammonium bromide (CTAB) as capping agent to control the particles morphology. The condition of the synthesis was obtained at 160 ºC for 24 hours with molar ratio of SrTiO3 and capping agent was 1 : 1. The X-ray diffraction (XRD) pattern shows that SrTiO3 adopts a perovskite structure with a higher intensity of 110 at 2q:32.33º and the crystallite size calculated from FWHM was found to be 41 nm. Fourier transform infrared (FTIR) spectrum shows a shift in particular absorption band attributed the interaction between SrTiO3 particles surface and the head group of CTAB molecules. Transmission electron microscopy (TEM) image shows the cubic-like particles of SrTiO3, this indicatesthat CTAB successfully functions as capping agent on the synthesis of SrTiO3.
- Subjects :
- Ammonium bromide
Materials science
capping agent, nanomaterials, nanocube, solvothermal, transmission electron
Infrared
Nanotechnology
General Chemistry
Biochemistry
Nanomaterials
Biomaterials
lcsh:Chemistry
chemistry.chemical_compound
chemistry
Chemical engineering
lcsh:QD1-999
Transmission electron microscopy
Absorption band
Environmental Chemistry
Molecule
Crystallite
Fourier transform infrared spectroscopy
Subjects
Details
- Language :
- English
- ISSN :
- 25030310 and 19079761
- Volume :
- 11
- Issue :
- 1
- Database :
- OpenAIRE
- Journal :
- Molekul
- Accession number :
- edsair.doi.dedup.....0afc7716ba6a455f757b0e6d7c5c0337