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A short, efficient synthesis of the chiral auxiliary (+)-8-phenylneomenthol

Authors :
Franco Fernández
José E. Rodríguez-Borges
Olga Caamaño
Xerardo García-Mera
Source :
CIÊNCIAVITAE, Scopus-Elsevier
Publication Year :
2000
Publisher :
Elsevier BV, 2000.

Abstract

(+)-8-Phenylneomenthol 2, the structure of which was confirmed by X-ray analysis of its 3,5-dinitrobenzoate, was efficiently prepared from commercially available (−)-8-phenylmenthol 3 by oxidation with the Sarett reagent, followed by L-Selectride reduction of the (+)-8-phenylmenthone 6 thus formed.

Details

ISSN :
00404039
Volume :
41
Database :
OpenAIRE
Journal :
Tetrahedron Letters
Accession number :
edsair.doi.dedup.....041b2baac3e53bfbea457a558f26932e