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Multikilogram Synthesis of a Potent Dual Bcl-2/Bcl-xL Antagonist. 1. Manufacture of the Acid Moiety and Development of Some Key Reactions

Authors :
Chloé Copin
François Barière
Anthony Craquelin
Solenn Janvier
Sylvain Lemaitre
Sébastien Samson
Sandrine Baillard
Olivier Russo
Christophe Hardouin
Stéphane Le Roux
Source :
Organic Process Research & Development. 24:652-669
Publication Year :
2019
Publisher :
American Chemical Society (ACS), 2019.

Abstract

Our efforts toward the process development of drug candidate 1 are described in a series of two papers. This manuscript focuses on the synthesis of kilogram quantities of acid precursor 2 to provid...

Details

ISSN :
1520586X and 10836160
Volume :
24
Database :
OpenAIRE
Journal :
Organic Process Research & Development
Accession number :
edsair.doi...........ed4125e9a1becd66e9e190e3d5397143
Full Text :
https://doi.org/10.1021/acs.oprd.9b00364