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Synthesis and Characterization of Linear Thermally Stable polyester contain Schiff Bases
- Source :
- Egyptian Journal of Chemistry.
- Publication Year :
- 2020
- Publisher :
- Egypts Presidential Specialized Council for Education and Scientific Research, 2020.
-
Abstract
- A copolymers are important compounds today because of their wide applications in various industrial and medical fields and in other fields. Therefore, the study of preparing many of these polymers has been studied. This research involved preparing linear polyester contain Schiff-base unit by interfacial polycondensation three type diacid chloride (Succinoyl Chloride, Adipoyl Chloride and sebacoyl Chloride) in a chloroform /water system employing phase transfer catalyst with monomer containing two hydroxyl which is derived from a 4-hydroxy aniline reacted with a 4-hydroxy benzaldehyde monomer. The monomer (EM1) and polyester (EM2, EM3, and EM4) were characterized by FTIR, 1H NMR, 13C NMR and TGA analysis. The polyester–Schiff base so obtained show good thermal stability.
- Subjects :
- chemistry.chemical_classification
Thermogravimetric analysis
020209 energy
Sebacoyl chloride
02 engineering and technology
Polymer
Adipoyl chloride
021001 nanoscience & nanotechnology
Chloride
Polyester
chemistry.chemical_compound
Monomer
chemistry
Polymer chemistry
0202 electrical engineering, electronic engineering, information engineering
medicine
0210 nano-technology
Phase-transfer catalyst
medicine.drug
Subjects
Details
- ISSN :
- 23570245
- Database :
- OpenAIRE
- Journal :
- Egyptian Journal of Chemistry
- Accession number :
- edsair.doi...........e3a5fe70357789004a5488823c9d9d60