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Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols

Authors :
Robert C. Buck
Alexander A. Marchione
Source :
Magnetic Resonance in Chemistry. 47:194-198
Publication Year :
2008
Publisher :
Wiley, 2008.

Abstract

A complete 1H, 19F, and 13C NMR assignment of a homologous series of polyfluorinated acids and alcohols is reported. These assignments were obtained chiefly through single and multiple-bond 1H–13C and 19F–13C correlation experiments (HSQC, HMBC). 19F NOESY experiments were required for assignment of two compounds with diastereotopic 19F nuclei in the CF2chain of the molecule. Copyright © 2008 John Wiley & Sons, Ltd.

Details

ISSN :
07491581
Volume :
47
Database :
OpenAIRE
Journal :
Magnetic Resonance in Chemistry
Accession number :
edsair.doi...........d25ceb1a1c858b3b14fa2af41bfc0035
Full Text :
https://doi.org/10.1002/mrc.2376