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An Efficient Method for Preparation of Chiral Arylmenthol Glyoxylates
- Source :
- Synthesis. 1998:1590-1592
- Publication Year :
- 1998
- Publisher :
- Georg Thieme Verlag KG, 1998.
-
Abstract
- Glyoxylates of three chiral alcohols were conveniently prepared by reaction of the alcohol with oxalyl chloride followed by reduction of the resulting alkoxy oxalyl chloride with tributyl- tin hydride. The products were isolated in 75-80% yield by straightforward flash chromatography.
Details
- ISSN :
- 1437210X and 00397881
- Volume :
- 1998
- Database :
- OpenAIRE
- Journal :
- Synthesis
- Accession number :
- edsair.doi...........a069fbedad6a238e853674594cac7523