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ChemInform Abstract: A Practical Synthesis of 4-Amino-2-methyl-10H-thieno[2,3-b][1,5]benzodiazepine

Authors :
Wei-Ming Xu
Ning Liu
Yu-Wei Chang
Ping-Ping Ye
Source :
ChemInform. 47
Publication Year :
2016
Publisher :
Wiley, 2016.

Abstract

The title compound (II), a key intermediate for the synthesis of the anti-psychotic drug olanzapine, is prepared by intramolecular cyclocondensation of [(nitrophenyl)amino]thiophenecarbonitrile (I) using tin powder and HCl a reducing system.

Details

ISSN :
09317597
Volume :
47
Database :
OpenAIRE
Journal :
ChemInform
Accession number :
edsair.doi...........94ec532c18eced3c1666a0b1afaaa753
Full Text :
https://doi.org/10.1002/chin.201652361