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Synthesis of Sulfonyl Azides via Lewis Base Activation of Sulfonyl Fluorides and Trimethylsilyl Azide
- Source :
- Synlett. 27:1840-1843
- Publication Year :
- 2016
- Publisher :
- Georg Thieme Verlag KG, 2016.
-
Abstract
- A protocol for the efficient conversion of sulfonyl fluorides into sulfonyl azides through Lewis base activation is described. The in situ generated sulfonyl azides are efficient diazo-transfer agents, affording diazo compounds and primary azides in excellent yields.
- Subjects :
- Sulfonyl
chemistry.chemical_classification
Primary (chemistry)
010405 organic chemistry
Organic Chemistry
010402 general chemistry
01 natural sciences
Medicinal chemistry
0104 chemical sciences
chemistry.chemical_compound
chemistry
Trimethylsilyl azide
Organic chemistry
Diazo
Lewis acids and bases
Sulfonyl fluoride
Subjects
Details
- ISSN :
- 14372096 and 09365214
- Volume :
- 27
- Database :
- OpenAIRE
- Journal :
- Synlett
- Accession number :
- edsair.doi...........8c66c7fe1c111041d08fa163f772624a