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Direct synthesis of monodispersed ZnO nanoparticles in an aqueous solution
- Source :
- Materials Letters. 61:690-693
- Publication Year :
- 2007
- Publisher :
- Elsevier BV, 2007.
-
Abstract
- Monodispersed ZnO nanoparticles with mesopores were successfully prepared via a simple route through the transformation of Zn(NH3)42+ precursor in the presence of sodium oleate and hydrazine at 80 °C with the pH of 8.5. Hydrazine and sodium oleate were used to control the size at 30–60 nm and to improve dispersion properties of ZnO nanoparticles. The samples were characterized by TEM, XRD, IR and TG-DTA, and the results suggest that the grains are composed of ZnO and a small quantity of oleate. The oleate plays an important role in preventing the ZnO nanoparticles from aggregating.
- Subjects :
- Materials science
Aqueous solution
Mechanical Engineering
Hydrazine
Inorganic chemistry
Condensed Matter Physics
chemistry.chemical_compound
Chemical engineering
chemistry
Zno nanoparticles
Mechanics of Materials
Sodium oleate
General Materials Science
Dispersion (chemistry)
Mesoporous material
Subjects
Details
- ISSN :
- 0167577X
- Volume :
- 61
- Database :
- OpenAIRE
- Journal :
- Materials Letters
- Accession number :
- edsair.doi...........86d7f10d2dcf5c62f3a54cec8703cf81