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Direct synthesis of monodispersed ZnO nanoparticles in an aqueous solution

Authors :
Xiaotang Lv
Xiaokun Ma
Minggang Li
Zichen Wang
Fang Sun
Lanqin Tang
Hari-Bala
Source :
Materials Letters. 61:690-693
Publication Year :
2007
Publisher :
Elsevier BV, 2007.

Abstract

Monodispersed ZnO nanoparticles with mesopores were successfully prepared via a simple route through the transformation of Zn(NH3)42+ precursor in the presence of sodium oleate and hydrazine at 80 °C with the pH of 8.5. Hydrazine and sodium oleate were used to control the size at 30–60 nm and to improve dispersion properties of ZnO nanoparticles. The samples were characterized by TEM, XRD, IR and TG-DTA, and the results suggest that the grains are composed of ZnO and a small quantity of oleate. The oleate plays an important role in preventing the ZnO nanoparticles from aggregating.

Details

ISSN :
0167577X
Volume :
61
Database :
OpenAIRE
Journal :
Materials Letters
Accession number :
edsair.doi...........86d7f10d2dcf5c62f3a54cec8703cf81