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A Convenient Synthesis of Chiral, Non-Racemic [4aS,8aR]-5,5,8a-Trimethyl Octahydro-2,2-(1,3-Dioxolane)-Naphthalene

Authors :
Beatriz Soares Machado Tenius
Evelyn Koeche Schroeder
Source :
Synthetic Communications. 30:1371-1378
Publication Year :
2000
Publisher :
Informa UK Limited, 2000.

Abstract

(-)-(4aS,8aR)-5,5-8a-trimethyl-trans-decaline 1 was prepared in a stereoespecific synthesis of 4 steps and 38% yield. The key-step involves an asymmetric Robinson annulation via Michael addition of chiral imine.

Details

ISSN :
15322432 and 00397911
Volume :
30
Database :
OpenAIRE
Journal :
Synthetic Communications
Accession number :
edsair.doi...........83f2e71091248d40847f5dd03182ac55