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Stable thiolate adducts of Rh2(OAc)4 – assembly of hexametallic Ni4Rh2 complexes

Authors :
Martin Börner
Berthold Kersting
Sara Schmorl
Source :
Dalton Transactions. 51:59-62
Publication Year :
2022
Publisher :
Royal Society of Chemistry (RSC), 2022.

Abstract

Thiolate adducts of dirhodium(II) tetraacetate have proven difficult to prepare. We isolated a stable, paramagnetic Ni4Rh2 adduct containing Ni-based metallothiolates bound in axial positions of the Rh24+ core. The adduct formation is accompanied by a change of the magnetic exchange interaction in the dinuclear Ni2 subunits.

Details

ISSN :
14779234 and 14779226
Volume :
51
Database :
OpenAIRE
Journal :
Dalton Transactions
Accession number :
edsair.doi...........712a2a269fabda8e513d41fec89bad3a
Full Text :
https://doi.org/10.1039/d1dt03509f