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Fast, quantitative nucleoside protection under solvent-free conditions

Authors :
Nicola Giri
Joseph S. Vyle
Caroline Bowen
Stuart L. James
Source :
Green Chemistry. 10:627
Publication Year :
2008
Publisher :
Royal Society of Chemistry (RSC), 2008.

Abstract

Persilylation of nucleoside hydroxyls was effected in quantitative yields under solvent-free conditions using a ball mill. In addition, one-pot persilylation and acylation of cytidine was performed as an exemplar reaction demonstrating the utility of solvent-free approaches to nucleoside chemistry.

Details

ISSN :
14639270 and 14639262
Volume :
10
Database :
OpenAIRE
Journal :
Green Chemistry
Accession number :
edsair.doi...........67f2e365b6930c7979430abb64db45f6
Full Text :
https://doi.org/10.1039/b801455h