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[Untitled]

Authors :
L. Apekis
R. Neffati
J. Rault
Source :
Journal of Thermal Analysis and Calorimetry. 54:741-752
Publication Year :
1998
Publisher :
Springer Science and Business Media LLC, 1998.

Abstract

It is shown that for porous systems filled with a solvent, if the temperature domains of crystallization and melting of the solvent are well separated, DSC technique, combined with suitably chosen thermal cycles, provides crystallization and melting curves which are independent of a) the mass of the material, b) the thermal contact between DSC pan and material and c) the thermal conductivity of the material. This method called DSC fractionation is applied to butyl rubber containing small water nodules. Thermoporosimetry is then applied to get the size distribution of mesoscopic solvent droplets.

Details

ISSN :
14182874
Volume :
54
Database :
OpenAIRE
Journal :
Journal of Thermal Analysis and Calorimetry
Accession number :
edsair.doi...........4f4498378b0cc2dafc95f284097b48e8
Full Text :
https://doi.org/10.1023/a:1010131601603