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Microwave-enhanced, solvent-free synthesis of singly and doubly13C-labelledtrans-cinnamic acid at the?- and?-carbon positions

Authors :
Sophia E. Hayes
Guibin Ma
Source :
Journal of Labelled Compounds and Radiopharmaceuticals. 47:895-901
Publication Year :
2004
Publisher :
Wiley, 2004.

Abstract

13C-labelled trans-cinnamic acid (3-phenyl-2-propenoic acid) has been synthesized in one step using benzaldehyde-carbonyl-13C and malonic acid-2-13C in the presence of ammonium acetate under microwave irradiation and solvent-free conditions. Copyright © 2004 John Wiley & Sons, Ltd.

Details

ISSN :
10991344 and 03624803
Volume :
47
Database :
OpenAIRE
Journal :
Journal of Labelled Compounds and Radiopharmaceuticals
Accession number :
edsair.doi...........4d51a722d75d989b00c366d7fd5c3beb
Full Text :
https://doi.org/10.1002/jlcr.878