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Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

Authors :
L. S. Skorokhod
S. Yu. Suikov
V. I. Pavlovskii
A. V. Pulya
S. L. Bogza
V. Kh. Kravtsov
I. I. Seifullina
Source :
Journal of Structural Chemistry. 59:497-501
Publication Year :
2018
Publisher :
Pleiades Publishing Ltd, 2018.

Abstract

Hydrazone [HydrHSal]∙Н2О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.

Details

ISSN :
15738779 and 00224766
Volume :
59
Database :
OpenAIRE
Journal :
Journal of Structural Chemistry
Accession number :
edsair.doi...........3ee40042ed4c9135a3c7220d96d7e773
Full Text :
https://doi.org/10.1134/s002247661802035x