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Convergent approach to intermediates used for the synthesis of the enediyne structure of the esperamicins and calicheamicins

Authors :
D.M. Vyas
Min Min Tun
Saulnier Mark G
J. F. Kadow
David R. Langley
Source :
Tetrahedron Letters. 30:3499-3500
Publication Year :
1989
Publisher :
Elsevier BV, 1989.

Abstract

The diynene lithium acetylide 5 adds to 2-siloxy-2-cyclohexenone 6 followed by silyl migration to produce ketone adduct 7 , an intermediate towards a simple Esperamicin core

Details

ISSN :
00404039
Volume :
30
Database :
OpenAIRE
Journal :
Tetrahedron Letters
Accession number :
edsair.doi...........3a843329b6e8a1ccfc283ab776baf7f9
Full Text :
https://doi.org/10.1016/s0040-4039(00)99423-1