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Determination of 3,4-methylenedioxymethamphetamine (MDMA) in Confiscated Tablets by High-Performance Liquid Chromatography (HPLC) with Diode Array Detector
- Source :
- Journal of Forensic Research.
- Publication Year :
- 2010
- Publisher :
- OMICS Publishing Group, 2010.
-
Abstract
- Chromatographic analysis by the HPLC technique with Diode Array Detector was employed for MDMA determination. A mobile phase of methanol/water (90:10v/v) allowed a peak signal for MDMA in 16 minutes. Optimized spectrophotometric signal was obtained at a wavelength of 240 nm. The analytical curve from 5.0 to 100.0ppm of MDMA was obtained, showing a linear correlation coefficient of 0.9997 and a detection limit of 2.94ppm. This methodology was employed at the dosage of confiscated samples of ecstasy in the Scientific Police Laboratory of Ribeirao Preto-SP city.
Details
- ISSN :
- 21577145
- Database :
- OpenAIRE
- Journal :
- Journal of Forensic Research
- Accession number :
- edsair.doi...........2665f9c699ab2482e38a6777570f6714