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Deformation-Induced Structural-Phase Transformations during Mechanosynthesis of Fe–Fullerite in Toluene
- Source :
- Physics of Metals and Metallography. 120:858-866
- Publication Year :
- 2019
- Publisher :
- Pleiades Publishing Ltd, 2019.
-
Abstract
- —X-ray diffraction, Mossbauer and Raman spectroscopy have been used to study structural phase transformations during mechanosynthesis of Fe–С60/70 in toluene with 20 and 25 at % С60/70 fullerite. The quantitative carbon content determines the phase composition of mechanocomposites. (Fe3C)D forms at 20 at % С60/70, whereas Fe7C3 and a paramagnetic phase form at 25 at % С60/70 at the initial stage of mechanical alloying. Free carbon is in an amorphous state in the sample. The formation mechanism of carbides and a paramagnetic component is discussed.
- Subjects :
- 010302 applied physics
Materials science
chemistry.chemical_element
Condensed Matter Physics
01 natural sciences
Carbide
Amorphous solid
symbols.namesake
Paramagnetism
chemistry
Phase (matter)
0103 physical sciences
Mössbauer spectroscopy
Materials Chemistry
symbols
Physical chemistry
Mechanosynthesis
010306 general physics
Raman spectroscopy
Carbon
Subjects
Details
- ISSN :
- 15556190 and 0031918X
- Volume :
- 120
- Database :
- OpenAIRE
- Journal :
- Physics of Metals and Metallography
- Accession number :
- edsair.doi...........18eaf66a7d988809526861e7cac90ea2