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Quantitative Analysis: The SEM/EDS Elemental Microanalysis k-ratio Procedure for Bulk Specimens, Step-by-Step
- Source :
- Scanning Electron Microscopy and X-Ray Microanalysis ISBN: 9781493966745
- Publication Year :
- 2017
- Publisher :
- Springer New York, 2017.
-
Abstract
- This module discusses the procedure used to perform a rigorous quantitative elemental microanalysis by SEM/EDS following the k-ratio/matrix correction protocol using the NIST DTSA-II software engine for bulk specimens. Bulk specimens have dimensions that are sufficiently large to contain the full range of the direct electron-excited X-ray production (typically 0.5–10 μm) as well as the range of secondary X-ray fluorescence induced by the propagation of the characteristic and continuum X-rays (typically 10–100 μm).
- Subjects :
- Materials science
Analytical chemistry
Microanalysis
Subjects
Details
- ISBN :
- 978-1-4939-6674-5
- ISBNs :
- 9781493966745
- Database :
- OpenAIRE
- Journal :
- Scanning Electron Microscopy and X-Ray Microanalysis ISBN: 9781493966745
- Accession number :
- edsair.doi...........04b4e1fd8ec0d68bea83e9eecfcfbbbf
- Full Text :
- https://doi.org/10.1007/978-1-4939-6676-9_20