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Reactions of Ethynylcarbenes Related to Solid-State Polymerization of 1-Phenyl-1,3-butadiyne

Authors :
Koga, Noboru
Matsumura, Masahiro
Noro, Masaki
Iwamura, Hiizu
Source :
Chemistry Letters; August 1991, Vol. 20 Issue: 8 p1357-1360, 4p
Publication Year :
1991

Abstract

1,8-Diphenyl-1,8-bis(diazo)-octa-4-ene-2,6-diyne was prepared and photolyzed to give 1-phenyl-1,3-butadiyne in high yield. Ethynylphenylcarbene and β-phenylethynylcarbene generated by photolysis in MTHF at 6 K are in equilibrium in which the latter predominates at 90 K.

Details

Language :
English
ISSN :
03667022 and 13480715
Volume :
20
Issue :
8
Database :
Supplemental Index
Journal :
Chemistry Letters
Publication Type :
Periodical
Accession number :
ejs64673439
Full Text :
https://doi.org/10.1246/cl.1991.1357