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Synthesis of Ti3SiC2-based composites by spark plasma sintering of preceramic papers

Authors :
Kashkarov, E B
Syrtanov, M S
Sedanova, E P
Ivashutenko, A S
Lider, A M
Travitzky, N
Source :
IOP Conference Series: Materials Science and Engineering; August 2019, Vol. 597 Issue: 1 p012058-012058, 1p
Publication Year :
2019

Abstract

This paper is devoted to fabrication of Ti3SiC2-based ceramic materials from preceramic paper using spark plasma sintering (SPS) method. The synthesis temperature and pressure were 1373-1473 K and 30 MPa, respectively. The phase composition, microstructure and elemental composition were analysed using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy, respectively. The effect of temperature on the sintering process as well as on the phase and microstructure of the sintered materials was investigated.

Details

Language :
English
ISSN :
17578981 and 1757899X
Volume :
597
Issue :
1
Database :
Supplemental Index
Journal :
IOP Conference Series: Materials Science and Engineering
Publication Type :
Periodical
Accession number :
ejs51889661