Observing thermomagnetic stability of nonideal magnetite particles: Good paleomagnetic recorders?

The thermomagnetic behavior of remanence‐induced magnetite (Fe3O4) particles in the pseudo‐single‐domain (PSD) size range (~0.1–10 µm), which dominate the magnetic signature of many rock lithologies, is investigated using off‐axis electron holography. Construction of magnetic induction maps allowed for the visualization of the vortex domain state in an individual Fe3O4grain (~200 nm in diameter) as a function of temperature. Acquisition of a series of electron holograms at 100°C intervals during in situ heating up to 700°C demonstrates the vortex state of the Fe3O4grain, in this instance, remains thermally stable close to its unblocking temperature and exhibits a similar in‐plane remanent state upon cooling; i.e., the particle is effectively behaving like a uniaxial single‐domain particle to temperatures near TC. Such particles are thought to be robust magnetic recorders. It is suggested that evidence for PSD behavior should therefore not preclude paleomagnetic investigation. Thermomagnetic stability of nonideal magnetite particlesVisualization of stability of vortex domain state with heatingParticles behave like uniaxial SD particles near to Curie temperature