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Hydrogen-bonding pyrrolic amide cleft anion receptors

Authors :
Gale, Philip A
Camiolo, Salvatore
Chapman, Christopher P
Light, Mark E
Hursthouse, Michael B
Source :
Tetrahedron Letters; July 2001, Vol. 42 Issue: 30 p5095-5097, 3p
Publication Year :
2001

Abstract

The use of simple 2,5-diamidopyrrole derivatives as anion receptors has been investigated. Reaction of 3,4-diphenylpyrrole-2,5-dicarboxylic acid chloride with n-butylamine or aniline has produced two new amidic cleft anion receptors 1and 2. The anion-coordination ability of these species has been determined by 1H NMR titration techniques. Crystal structures of 1and 2have been elucidated, revealing a continuous hydrogen bonding network formed by 1and dimerization of 2via NH⋯O and CH⋯O hydrogen bonds.

Details

Language :
English
ISSN :
00404039
Volume :
42
Issue :
30
Database :
Supplemental Index
Journal :
Tetrahedron Letters
Publication Type :
Periodical
Accession number :
ejs41901568
Full Text :
https://doi.org/10.1016/S0040-4039(01)00896-6