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A Convenient Synthesis and a NMR Study of the Diammoniate of Diborane
- Source :
- Chemistry - A European Journal; March 2012, Vol. 18 Issue: 12 p3490-3492, 3p
- Publication Year :
- 2012
-
Abstract
- DADB synthesis: The diammoniate of diborane (DADB) was synthesized in a new metathesis reaction between the diammoniate of monochloroborane and potassium borohydride in liquid ammonia (see scheme). 1H and 11B NMR spectra of DADB are reported. The stability in THF was examined by variable‐temperature 11B NMR spectroscopy.
Details
- Language :
- English
- ISSN :
- 09476539 and 15213765
- Volume :
- 18
- Issue :
- 12
- Database :
- Supplemental Index
- Journal :
- Chemistry - A European Journal
- Publication Type :
- Periodical
- Accession number :
- ejs27007146
- Full Text :
- https://doi.org/10.1002/chem.201103693