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Über die Darstellung von Trilithium-trisulfimid (Trilithium-1,3,5,2,4,6-trithiatriazin-1,1,3,3,5,5-hexaoxid) und die thermische Zersetzung einiger Salze des Trisulfimids
- Source :
- Monatshefte für Chemie / Chemical Monthly; July 1973, Vol. 104 Issue: 4 p1131-1138, 8p
- Publication Year :
- 1973
-
Abstract
- Trilithiumhexaoxocyclotrithiazane<superscript>*</superscript> (trilithiumtrisulfimid) has been prepared for the first time by reaction of triammoniumtrisulfimid with LiOH in a solid state reaction and by using high boiling alcohols as reaction medium. The thermolysis of different salts of trisulfimid (Na-, K-, Li-, Ag-, NH<subscript>4</subscript>-salt) has been studied by thermoanalytical methods in the region between 25–500 dC. The course of decomposition of these compounds is discussed by IR and chromatographic measurements.
Details
- Language :
- English
- ISSN :
- 00269247 and 14344475
- Volume :
- 104
- Issue :
- 4
- Database :
- Supplemental Index
- Journal :
- Monatshefte für Chemie / Chemical Monthly
- Publication Type :
- Periodical
- Accession number :
- ejs16239244
- Full Text :
- https://doi.org/10.1007/BF00903932