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Combined Application of QEM-SEM and Hard X-ray Microscopy to Determine Mineralogical Associations and Chemical Speciation of Trace Metals.

Authors :
Gräfe, Markus
Landers, Matthew
Tappero, Ryan
Austin, Peter
Gan, Bee
Grabsch, Alton
Klauber, Craig
Source :
Journal of Environmental Quality; May/Jun2011, Vol. 40 Issue 3, p767-783, 17p
Publication Year :
2011

Abstract

The article presents a study on the combined application of quantitative evaluation of mineralogy by scanning electron microscope (QEM-SEM) and hard X-ray microscopy to determine mineralogical associations and chemical speciation of trace metals in the U.S. It notes the reliance of successful trace metal speciation in heterogeneous matrices on a combination of techniques including spectroscopy, microscopy and wet chemical and physical experiments. It highlights the detailed insights provided by the QEM-SEM with micro-focused X-ray diffraction into the composition of mineral assemblages and their effect on trace metal speciation.

Details

Language :
English
ISSN :
00472425
Volume :
40
Issue :
3
Database :
Supplemental Index
Journal :
Journal of Environmental Quality
Publication Type :
Academic Journal
Accession number :
60761820
Full Text :
https://doi.org/10.2134/jeq2010.0214