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Copper(I)-Mediated 1,2-Metallate Rearrangements of 1-Metallated Glycals.

Authors :
Jarowicki, Krzysztof
Kocie&neacute;ski, Philip
Komsta, Zofia
Wojtasiewicz, Anna
Source :
Synthesis; 2012, Vol. 2012 Issue 6, p946-952, 7p
Publication Year :
2012

Abstract

1,2-Metallate rearrangements involving reaction of 1-metallated glycals with organolithium reagents under copper(I) me-diation give alkenylpolyol chains in 45-91% yield (19 examples). The reaction was applied to a formal synthesis of KRN7000 as well as a synthesis of a δ<superscript>5,6</superscript>-ceramide derivative. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00397881
Volume :
2012
Issue :
6
Database :
Complementary Index
Journal :
Synthesis
Publication Type :
Academic Journal
Accession number :
75196156
Full Text :
https://doi.org/10.1055/s-0031-1289721