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Desymmetrization of Hepta-1,6-dien-4-ol by Prins Reaction and Subsequent Cross-Metathesis: Access to Diospongine A Homologues.

Authors :
Raffier, Ludovic
Izquierdo, Frédéric
Piva, Olivier
Source :
Synthesis; 2011, Vol. 2011 Issue 24, p4037-4044, 8p
Publication Year :
2011

Abstract

A new tetrahydropyran scaffold has been efficiently prepared by Prins reaction between hepta-1,6-dien-4-ol and benzaldehyde. Subsequent functionalizations were further achieved by Mitsunobu reaction and/or by the way of cross-metathesis/Wacker oxidation sequence to deliver diospongin A analogues. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00397881
Volume :
2011
Issue :
24
Database :
Complementary Index
Journal :
Synthesis
Publication Type :
Academic Journal
Accession number :
69598035
Full Text :
https://doi.org/10.1055/s-0031-1289588