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One-Pot Preparation of 2,5-Dichloro-4'-phenyloxybenzophenone.
- Source :
- Synthetic Communications; 2011, Vol. 41 Issue 2, p255-261, 7p
- Publication Year :
- 2011
-
Abstract
- Friedel-Crafts-type acylation of phenyl ether with 2,5-dichlorobenzoic acid could be accomplished in a single step using trifluoroacetic anhydride and phosphoric acid. The method gave a greater yield (78%) than the conventional two-step process (71%) of acid chloride generation followed by aluminum trichloride-mediated acylation. [ABSTRACT FROM AUTHOR]
- Subjects :
- ORGANIC synthesis
ANHYDRIDES
PHOSPHORIC acid
ACYLATION
ALUMINUM
CHLORIDES
BENZOIC acid
Subjects
Details
- Language :
- English
- ISSN :
- 00397911
- Volume :
- 41
- Issue :
- 2
- Database :
- Complementary Index
- Journal :
- Synthetic Communications
- Publication Type :
- Academic Journal
- Accession number :
- 56043394
- Full Text :
- https://doi.org/10.1080/00397910903534056