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Preparation of nanosized metal-oxide ultrafine powders by atomizing-combustion technique.

Authors :
Chen, Shizhu
Yin, Zhimin
Source :
Journal of Central South University of Technology; Nov1998, Vol. 5 Issue 2, p79-81, 3p
Publication Year :
1998

Abstract

The nano-sized metal-oxide ultrafine powders of the low-melting-point metals can be prepared rapidly using a new atomizing - combustion technique by which the superheated metal melt was atomized with a ceramic atomizing-burner first through the medium of high pressure oxygen, then the metal fog burned up in a combustion chamber. Based on the experiments, nano-sized SnO<subscript>2</subscript>, In<subscript>2</subscript>O<subscript>3</subscript> and Bi<subscript>2</subscript>O<subscript>3</subscript> powders were obtained successfully by atomizing-combustion technique. The mechanism and process parameters of the technique were discussed. The phase structure and the microstructure of these metal-oxide ultrafine powders were studied by XRD and TEM respectively. The biggest size of grain was less than 50 nm, and 1 kg metal-oxide ultrafine powder can be prepared in only 45–48 seconds. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
10059784
Volume :
5
Issue :
2
Database :
Complementary Index
Journal :
Journal of Central South University of Technology
Publication Type :
Academic Journal
Accession number :
49621506
Full Text :
https://doi.org/10.1007/s11771-998-0040-9