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Synthesis, Spectroscopic (FT-IR, ¹H, 13C, Mass Spectrometry), and Biological Investigation of Five-Coordinated Germanium-Substituted Tricyclohexyl Antimony Dipropionates: Crystal Structure of Tricyclohexylantimony Dibromide.

Authors :
Khosa, Muhammad Kaleem
Mazhar, Muhammad
Ali, Saqib
Molloy, Kieran C.
Dastgir, Sarim
Shaheen, Farkhanda
Source :
Turkish Journal of Chemistry; 2006, Vol. 30 Issue 6, p731-743, 13p
Publication Year :
2006

Abstract

A series of five-coordinated germanium-substituted tricyclohexylantimony dipropionates have been synthesized and characterized by different instrumental techniques, such as elemental analyses, FT-IR, multinuclear NMR (¹H, <superscript>13</superscript>C) and mass spectrometry. These compounds have also been screened against different microbes and they showed good activity against different bacteria that was comparable to the reference drugs. The crystal structure of the precursor (C<subscript>6</subscript>H<subscript>11</subscript>)<subscript>3</subscript>SbBr<subscript>2</subscript> is reported here, which showed that the antimony atom in an asymmetric unit exists in trigonal bipyramidal geometry, having space group C2/c with the monoclinic crystal system. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
13000527
Volume :
30
Issue :
6
Database :
Complementary Index
Journal :
Turkish Journal of Chemistry
Publication Type :
Academic Journal
Accession number :
24309934