Back to Search Start Over

cis-Bis[(3-amino­prop­yl)dimethyl­phosphine-κ2 N, P]palladium(II) dichloride methanol solvate.

Authors :
Suzuki, Takayoshi
Hasegawa, Atsushi
Yamaguchi, Hiroshi
Kashiwabara, Kazuo
Takagi, Hideo D.
Source :
Acta Crystallographica: Section C (Wiley-Blackwell); Oct2006, Vol. 62 Issue 10, pm461-m463, 1p, 2 Diagrams, 2 Charts
Publication Year :
2006

Abstract

In the title compound, cis-[Pd(C<subscript>5</subscript>H<subscript>14</subscript>NP)<subscript>2</subscript>]Cl<subscript>2</subscript>·CH<subscript>4</subscript>O, the coordination geometry around the Pd<superscript>II</superscript> center is distorted square planar, with a cis-P<subscript>2</subscript>N<subscript>2</subscript> configuration of the two chelating (3-aminopropyl)dimethylphosphine (pdmp) ligands. The six-membered pdmp chelate rings adopt chair conformations, and pairing of the chairs designates the complex cation as a (C<subscript>s</subscript>)-chair<subscript>2</subscript> conformer. The distances between the Pd<superscript>II</superscript> center and the Cl<superscript>-</superscript> anions are greater than 4.5 Å, indicating no obvious interaction. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
01082701
Volume :
62
Issue :
10
Database :
Complementary Index
Journal :
Acta Crystallographica: Section C (Wiley-Blackwell)
Publication Type :
Academic Journal
Accession number :
22554670
Full Text :
https://doi.org/10.1107/S0108270106023596