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Liquid-phase extraction combined with X-ray fluorescence spectrometry for the elemental determination.
- Source :
- Applied Spectroscopy Reviews; 2023, Vol. 58 Issue 9, p610-628, 19p
- Publication Year :
- 2023
-
Abstract
- X-ray fluorescence spectrometry (XRF) has been widely used for multi-element determination in various samples. However, when trace level determination is required, separation and preconcentration procedures are often used as a step before detection to avoid or reduce interferences and to increase sensitivity. Liquid-phase extraction (LPE) is one of the most well-known and applied pretreatment techniques associated with atomic spectrometry due to its simplicity, speed, and ease of automation. A review of methods involving LPE combined with XRF is presented. Methods described in the literature are discussed, involving conventional LPE and the three main categories of liquid-phase microextraction (LPME): single-drop microextraction (SDME), dispersive liquid–liquid microextraction (DLLME), and hollow fiber liquid-phase microextraction (HF-LPME). Characteristics of the methods are presented, considering experimental aspects, analytical features, advantages, and disadvantages. In addition, trends in the association between LPME techniques and XRF are presented. [ABSTRACT FROM AUTHOR]
- Subjects :
- FLUORESCENCE spectroscopy
X-ray fluorescence
HOLLOW fibers
SPECTROMETRY
Subjects
Details
- Language :
- English
- ISSN :
- 05704928
- Volume :
- 58
- Issue :
- 9
- Database :
- Complementary Index
- Journal :
- Applied Spectroscopy Reviews
- Publication Type :
- Academic Journal
- Accession number :
- 172442530
- Full Text :
- https://doi.org/10.1080/05704928.2022.2113537