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PVP/Highly Dispersed AgNPs Nanofibers Using Ultrasonic-Assisted Electrospinning.

Authors :
Zhu, Li
Zhu, Wanying
Hu, Xin
Lin, Yingying
Machmudah, Siti
Wahyudiono
Kanda, Hideki
Goto, Motonobu
Source :
Polymers (20734360); Feb2022, Vol. 14 Issue 3, p599, 1p
Publication Year :
2022

Abstract

Silver nanoparticles (AgNPs) are novel materials with antibacterial, antifungal, and antiviral activities over a wide range. This study aimed to prepare polyvinylpyrrolidone (PVP) electrospinning composites with uniformly distributed AgNPs. In this study, starch-capped ~2 nm primary AgNPs were first synthesized using Atmospheric pressure Pulsed Discharge Plasma (APDP) at AC 10 kV and 10 kHz. Then, 0.6 wt.% AgNPs were mixed into a 10 wt.% PVP ethanol-based polymer solution and coiled through an Ultrasonic-assisted Electrospinning device (US-ES) with a 50 W and 50 kHz ultrasonic generator. At 12 kV and a distance of 10 cm, this work successfully fabricated AgNPs-PVP electrospun fibers. The electrospun products were characterized using Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), High-Resolution TEM (HR-TEM), Fourier Transform Infrared Spectroscopy (FT-IR), X-ray Diffraction (XRD), Thermogravimetric (TG), and X-ray Photoelectron Spectroscopy (XPS) methods. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
20734360
Volume :
14
Issue :
3
Database :
Complementary Index
Journal :
Polymers (20734360)
Publication Type :
Academic Journal
Accession number :
155269583
Full Text :
https://doi.org/10.3390/polym14030599