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Generation and simple characterization of flat, liquid jets.

Authors :
Menzi, Samuel
Knopp, Gregor
Al Haddad, Andre
Augustin, Sven
Borca, Camelia
Gashi, Dardan
Huthwelker, Thomas
James, Daniel
Jin, Jiaye
Pamfilidis, Georgios
Schnorr, Kirsten
Sun, Zhibin
Wetter, Reto
Zhang, Qiang
Cirelli, Claudio
Source :
Review of Scientific Instruments; Oct2020, Vol. 91 Issue 10, p1-10, 10p
Publication Year :
2020

Abstract

We present an approach to determine the absolute thickness profile of flat liquid jets, which takes advantage of the information of thin film interference combined with light absorption, both captured in a single microscopic image. The feasibility of the proposed method is demonstrated on our compact experimental setup used to generate micrometer thin, free-flowing liquid jet sheets upon collision of two identical laminar cylindrical jets. Stable operation was achieved over several hours of the flat jet in vacuum (10<superscript>−4</superscript> mbar), making the system ideally suitable for soft x-ray photon spectroscopy of liquid solutions. We characterize the flat jet size and thickness generated with two solvents, water and ethanol, employing different flow rates and nozzles of variable sizes. Our results show that a gradient of thickness ranging from a minimal thickness of 2 µm to over 10 µm can be found within the jet surface area. This enables the tunability of the sample thickness in situ, allowing the optimization of the transmitted photon flux for the chosen photon energy and sample. We demonstrate the feasibility of x-ray absorption spectroscopy experiments in transmission mode by measuring at the oxygen K-edge of ethanol. Our characterization method and the description of the experimental setup and its reported performance are expected to expand the range of applications and facilitate the use of flat liquid jets for spectroscopy experiments. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00346748
Volume :
91
Issue :
10
Database :
Complementary Index
Journal :
Review of Scientific Instruments
Publication Type :
Academic Journal
Accession number :
146790129
Full Text :
https://doi.org/10.1063/5.0007228