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Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer.
- Source :
- Journal of Materials Science; Sep2020, Vol. 55 Issue 25, p11213-11225, 13p, 1 Black and White Photograph, 3 Diagrams, 1 Chart, 7 Graphs
- Publication Year :
- 2020
-
Abstract
- Poly(N-isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi<subscript>2</subscript>O<subscript>3</subscript> (PNIPAM/Bi<subscript>2</subscript>O<subscript>3</subscript>) was prepared by a novel one-step continuous microwave method. This new method is efficient and convenient. The as-prepared PNIPAM/Bi<subscript>2</subscript>O<subscript>3</subscript> was very sensitive to temperature and pH, and the degradation rate in the environment of 25 °C and pH = 9 was 3.87 times than that in the environment of 45 °C and pH = 5. While Bi<subscript>2</subscript>O<subscript>3</subscript> is under the above various environmental conditions, its degradation rate did not change obviously. More interestingly, the introduction of PNIPAM and one-step continuous microwave method was beneficial to the transformation of Bi<subscript>2</subscript>O<subscript>3</subscript> from no specific shape to rodlike morphology without changing its crystal structure. This work not only developed a new one-step continuous microwave synthesis method, but also opened up new ideas for the controllability requirements of materials in special environment. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 00222461
- Volume :
- 55
- Issue :
- 25
- Database :
- Complementary Index
- Journal :
- Journal of Materials Science
- Publication Type :
- Academic Journal
- Accession number :
- 143700370
- Full Text :
- https://doi.org/10.1007/s10853-020-04799-w