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The Right Light: De Novo Design of a Robust Modular Photochemical Reactor for Optimum Batch and Flow Chemistry.
- Source :
- ChemPhotoChem; Jan2020, Vol. 4 Issue 1, p45-51, 7p
- Publication Year :
- 2020
-
Abstract
- Having identified inconsistencies when repeating literature examples of photochemical transformations and difficulties recreating experimental setups, we devised several criteria that an ideal lab‐scale reactor should achieve. Herein, we introduce a versatile photoreactor for high‐throughput screening, preparative‐scale batch reactions and continuous processing, all with a single light source. The reactor utilizes interchangeable arrays of pseudo‐monochromatic high‐power LEDs in a range of synthetically useful wavelengths, combined with excellent temperature control. Moreover, light intensity can be modulated in an accurate and straightforward manner. This system has subsequently been tested on a range of literature methodologies. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 23670932
- Volume :
- 4
- Issue :
- 1
- Database :
- Complementary Index
- Journal :
- ChemPhotoChem
- Publication Type :
- Academic Journal
- Accession number :
- 141289397
- Full Text :
- https://doi.org/10.1002/cptc.201900203